ISO INTERNATIONAL STANDARD 13678 Third edition 2010-12-01 Petroleum and natural gas industries - Evaluation and testing of thread compounds for use with casing, tubing, line pipe and drill stem elements Industries du pétrole et du gaz naturel - Evaluation et essais des graisses pour filetage utilisées pour les tubes de cuvelage, les tubes de production, les tubes de conduites et les élements de garnitures de forage Reference number ISO 13678:2010(E) @ ISO 2010 y IHS unde ted without license from IHS Not for Resale ISO 13678:2010(E) PDF disclaimer This PDF file may contain embedded typefaces. In accordance with Adobe's licensing policy, this file may be printed or viewed but shall not be edited unless the typefaces which are embedded are licensed to and installed on the computer performing the editing. In accepts no liability in this area. Adobe is a trademark of Adobe Systems Incorporated. Details of the software products used to create this PDF file can be found in the General Info relative to the file; the PDF-creation parameters were optimized for printing. Every care has been taken to ensure that the file is suitable for use by IsO member bodies. In COPYRIGHT PROTECTED DOCUMENT @ISO2010 All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means, electronic or mechanical, including photocopying and microfilm, without permission in writing from either isO at the address below or ISO's member body in the country of the requester. ISO copyright office Case postale 56 . CH-1211 Geneva 20 Tel. + 41 22 749 01 11 Fax + 41 22 749 09 47 E-mail [email protected] Web www.iso.org Published in Switzerland Copyrgh Interatinal organization for Standardization @ ISO 2010 - All rights reserved I without license from IHS Not for Resale ISO 13678:2010(E) Contents Page Foreword Introductior 1 Scope 2 2.1 Conformance. Dual citing of normative references .. 2.2 Units of measurement.... 3 Normative references. 4 Terms and definitions. 5 Thread compound characteristics. 5.1 Product characteristics.... 5.2 Physical and chemical characteristics. 6 Threadcompoundperformanceproperties... 6.1 Small-scaletest 6.2 Frictional properties. .8 6.3 Extremesurfacecontactpressure(gallresistance)propertiesforcasing,tubingandline pipe. 6.4 Fluid sealing properties for casing, tubing and line pipe . 10 7 Quality assurance and control. 10 8 Marking requirements. 8.1 Marking.... 11 8.2 Labelling.... Annex A (informative) API modified thread compound ... Annex B (normative) Casing, tubing and line pipe reference standard formulation. ..16 Annex C (normative) Penetration test ... Annex D (normative) Evaporation test ... ...19 Annex E (normative) Oil separation test .. 20 Annex F (normative) Application/adherence test. 21 Annex G (normative) Gas evolution test.. 22 Annex H (normative) Water leaching test.... Annex I (informative) Frictional properties test .. Annex J (informative) Extreme surface contact pressure (galling) test for casing, tubing and line pipe.... .39 Annex K (informative) Fluid sealing test for casing, tubing and line pipe... ..40 Annex L (informative) Corrosion inhibition tests , ..43 Annex M (informative) Compound high-temperature stability test. ..44 Bibliography 45 CopyrghtInternational OrganizaionStadardizaonghtsreserved ii ut license from IHS Not for Resale